• 专利标题:   Preparation of graphene involves adding prepared expandable graphite to organic foaming agent solution and allowing to standstill, stirring at room temperature, ultrasonically treating, cooling and drying product.
  • 专利号:   CN103964426-A, CN103964426-B
  • 发明人:   JIN C, YANG X
  • 专利权人:   SUZHOU SDIK NEW MATERIAL TECHNOLOGY, SUZHOU SIDIKE NEW MATERIALS SCI TECHNO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103964426-A 06 Aug 2014 C01B-031/04 201469 Pages: 6 Chinese
  • 申请详细信息:   CN103964426-A CN10205625 15 May 2014
  • 优先权号:   CN10205625

▎ 摘  要

NOVELTY - Natural flaky graphite is dispersed in mixed solution of ethanol and concentrated nitric acid in volume ratio of 50:1-50:10, to obtain 0.005-0.05 g/mL suspension. The suspension is hydrothermally reacted at 80-160 degrees C for 6-48 hours, cooled, filtered, precipitated, washed and dried, to obtain expandable graphite. The expandable graphite is added to organic foaming agent solution and allowed to standstill for 30 minutes to 3 hours, stirred at room temperature for 1-5 hours, ultrasonically treated for 13-60 minutes, cooled and dried in vacuum, to obtain graphene. USE - Preparation of graphene (claimed). ADVANTAGE - The method efficiently and economically provides graphene without adding stabilizer.