• 专利标题:   Preparing hexagonal metal organic composite material involves mixing carboxylated graphene in deionized water with stirring to prepare aqueous dispersion.
  • 专利号:   CN105688867-A, CN105688867-B
  • 发明人:   FENG C, LIU L, LIU S, WANG T, ZHANG F
  • 专利权人:   UNIV SHANGQIU
  • 国际专利分类:   B01J020/22, B01J020/28, B01J020/30
  • 专利详细信息:   CN105688867-A 22 Jun 2016 B01J-020/30 201661 Chinese
  • 申请详细信息:   CN105688867-A CN10135195 10 Mar 2016
  • 优先权号:   CN10135195

▎ 摘  要

NOVELTY - Hexagonal metal organic composite material preparation involves mixing 1-4 ml carboxylated graphene in 7-10 ml deionized water with stirring for 4-6 hours to prepare aqueous dispersion. The prepared aqueous dispersion is mixed with 2.5-4 mmol copper nitrate and 10-5 ml ethanol in stainless steel high pressure reactor at 100-120 degrees C for 4-6 hours under ultrasonic dispersion to prepare mixed dispersion. The prepared mixed dispersion is mixed with 1-3 mmol trimesic acid in stainless steel autoclave at 100-120 degrees C for 16-20 hours. USE - Method for preparing hexagonal metal organic composite material (claimed). ADVANTAGE - The method prepares the hexagonal metal organic composite material in a simple, cost-effective and eco-friendly manner under mild reaction conditions. DETAILED DESCRIPTION - Hexagonal metal organic composite material preparation involves mixing 1-4 ml carboxylated graphene in 7-10 ml deionized water with stirring for 4-6 hours to prepare aqueous dispersion. The prepared aqueous dispersion is mixed with 2.5-4 mmol copper nitrate and 10-5 ml ethanol in stainless steel high pressure reactor at 100-120 degrees C for 4-6 hours under ultrasonic dispersion to prepare mixed dispersion. The prepared mixed dispersion is mixed with 1-3 mmol trimesic acid in stainless steel autoclave at 100-120 degrees C for 16-20 hours, where the formed product is filtered and washed with deionized water and absolute ethanol, and then dried in vacuum to obtain the hexagonal metal organic composite material. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic scanning electron microscope photograph of the hexagonal metal organic composite material.