• 专利标题:   Modified graphene oxide material preparation polyphenylene sulfide material, involves adding graphite powder to mixed acid solution with stirring to obtain suspension, and then placing prepared suspension in parallel electric field.
  • 专利号:   CN109019584-A
  • 发明人:   ZHANG H, ZHANG Y
  • 专利权人:   SICHUAN LIZHI JIUCHUANG INTELLECTUAL PRO
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN109019584-A 18 Dec 2018 C01B-032/198 201917 Pages: 7 Chinese
  • 申请详细信息:   CN109019584-A CN11033565 05 Sep 2018
  • 优先权号:   CN11033565

▎ 摘  要

NOVELTY - Modified graphene oxide material preparation involves adding graphite powder to the mixed acid solution with stirring to obtain a suspension, placing the prepared suspension in a parallel electric field after adding potassium permanganate powder with stirring to obtain another suspension. The obtained suspension is cooled at room temperature, and then mixed with hydrogen peroxide solution and hydrochloric acid solution to obtain a third suspension. The obtained third suspension is washed with deionized water, filtered, and then added to 50% aqueous solution of ethanol to disperse to obtain a fourth suspension. A modifier is added to the obtained fourth suspension under heating for obtaining a fifth suspension. USE - Method for preparing modified graphene oxide material for a polyphenylene sulfide material (claimed). ADVANTAGE - The method prepares the modified graphene oxide material in a simple, cost-effective and eco-friendly manner. DETAILED DESCRIPTION - The fifth suspension is washed with deionized water and centrifuging to obtain a precipitate, where the precipitate is vacuum dried under constant temperature conditions to obtain modified graphene oxide for polyphenylene sulfide material. The mixed acid solution is prepared by mixing a sulfuric acid solution and nitric acid solution. The modifier is a mixture of sulfonic acid imidazole, phenol and zinc dialkyl dithiophosphate.