• 专利标题:   Preparing vanadium dioxide and graphene oxide composite material by preparing vanadyl glycol, placing vanadyl glycol solution, graphene oxide solution and water into hydrothermal reaction kettle and reacting.
  • 专利号:   CN112242512-A
  • 发明人:   YAO J, LI D, LIU B, PENG S
  • 专利权人:   CHENGDU ADVANCED METALLIC MATERIALS IND
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/48, H01M004/583
  • 专利详细信息:   CN112242512-A 19 Jan 2021 H01M-004/36 202114 Pages: 6 Chinese
  • 申请详细信息:   CN112242512-A CN11112484 16 Oct 2020
  • 优先权号:   CN11112484

▎ 摘  要

NOVELTY - Method for preparing vanadium dioxide and graphene oxide composite material involves (a) preparing vanadyl glycol by mixing the vanadium source and ethylene glycol in a mass ratio of 1:(1-20), stirring and reacting at 30-200° C for 2-12 hours, cooling to normal temperature and filtering to obtain glycol vanadyl solution and (b) placing the vanadium ethylene glycol solution, graphene oxide solution, and deionized water into the hydrothermal reaction kettle in a volume ratio of 1:1:3-10, reacting at 120-220° C for 12-24 hours, cooling, immersing the reaction product in deionized water for 24 hours, and freeze-drying to obtain the product. USE - Method for preparing vanadium dioxide and graphene oxide composite material. ADVANTAGE - The method is short in reaction process, and simple in operation, does not produce toxic and harmful substances, is economical and environmentally-friendly, does not require large-scale equipment and harsh medium atmosphere and achieves large-scale industrial production.