• 专利标题:   Preparing nitrogen-doped graphene at large scale, by adding nitrogen-containing precursor and carbon-containing precursor to high pressure kettle, reacting and treating mixture using hydrochloric acid solution, and drying product.
  • 专利号:   CN102718206-A
  • 发明人:   BAO X, DENG D, PAN X
  • 专利权人:   CHINESE ACAD SCI DALIAN CHEM PHYS INST
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102718206-A 10 Oct 2012 C01B-031/04 201326 Chinese
  • 申请详细信息:   CN102718206-A CN10076806 29 Mar 2011
  • 优先权号:   CN10076806

▎ 摘  要

NOVELTY - Preparing nitrogen-doped graphene at large scale, involves (a) adding nitrogen-containing precursor and carbon-containing precursor under the protection of inert gas to high pressure kettle, (b) placing the kettle for 1-20 hours at 150-500 degrees C, (c) treating the obtained product using hydrochloric acid solution (5-37.5 %mass) for 3-5 hours, and washing the obtained product using water and ethanol, respectively until the product becomes neutral, and (d) extracting the obtained product, mixing and drying the obtained product to obtain the nitrogen-doped graphene. USE - The method is useful for preparing nitrogen-doped graphene at large scale. ADVANTAGE - The method is simple, and easy to operate and control.