• 专利标题:   Preparing polypyrrole coated sulfur nano particle-graphene fiber non-woven fabric composite material for use in the lithium-sulfur battery, involves preparing sodium thiosulfate, adding acid solution, stirring and reacting, taking precipitate and cleaning, and preparing coated sulfur nanoparticles.
  • 专利号:   CN114551852-A
  • 发明人:   ZHANG Y, HUANG L, XIA X
  • 专利权人:   UNIV CHINA ELECTRONIC SCI TECHNOLOGY
  • 国际专利分类:   D01F009/08, H01M010/052, H01M010/42, H01M004/38, H01M004/62, H01M004/66
  • 专利详细信息:   CN114551852-A 27 May 2022 H01M-004/38 202269 Chinese
  • 申请详细信息:   CN114551852-A CN10181927 25 Feb 2022
  • 优先权号:   CN10181927

▎ 摘  要

NOVELTY - Preparing polypyrrole coated sulfur nano particle-graphene fiber non-woven fabric composite material involves preparing the sodium thiosulfate and the surface-active agent in water and stirring, adding acid solution, stirring and reacting, taking the precipitate and cleaning to obtain the nano sulfur particles, preparing coated sulfur nanoparticles the nano sulfur particles constant temperature water bath stirring, adding auxiliary solvent and initiator after secondary stirring, then adding pyrrole three times stirring, at last, collecting the product and washing, dry polypyrrole coated sulfur nanoparticles, preparing coated sulfur nano particle-oxidized graphene under the grinding condition, the polypyrrole coated sulfur nanoparticle is added to the graphene solution, obtaining the dispersion after spinning, obtaining polypyrrole coated sulfur nano- particle-graphene short fiber, preparing coated sulfur nano particle-oxidized graphene fiber non-woven fabric composite material. USE - Method for preparing polypyrrole coated sulfur nano particle-graphene fiber non-woven fabric composite material for use in the lithium-sulfur battery positive electrode material. ADVANTAGE - The method has good mechanical performance, excellent conductivity, and flexibility, as a self-supporting lithium-sulfur battery positive electrode material has high specific capacity and excellent cycle magnification performance. DETAILED DESCRIPTION - Preparing polypyrrole coated sulfur nano particle-graphene fiber non-woven fabric composite material involves preparing the sodium thiosulfate and the surface-active agent in water and stirring, adding acid solution, stirring and reacting, taking the precipitate and cleaning to obtain the nano sulfur particles, preparing coated sulfur nanoparticles the nano sulfur particles constant temperature water bath stirring, adding auxiliary solvent and initiator after secondary stirring, then adding pyrrole three times stirring, at last, collecting the product and washing, dry polypyrrole coated sulfur nanoparticles, preparing coated sulfur nano particle-oxidized graphene under the grinding condition, the polypyrrole coated sulfur nanoparticle is added to the graphene solution, obtaining the dispersion after spinning, obtaining polypyrrole coated sulfur nano- particle-graphene short fiber, preparing coated sulfur nano particle-oxidized graphene fiber non-woven fabric composite material, the polypyrrole coated sulfur nano particle-oxidized graphene the short fiber for filtering, dry, washing and secondary dry, and preparing the polypyrrole coated sulfur nano particle-oxidized graphene fiber non-woven fabric composite material.