• 专利标题:   Preparation of anti-aging UV curing adhesive involves vacuum-drying graphene, adding acetone, stirring, adding titanium tetrachloride and magnesium chloride, stirring, ball milling and grinding.
  • 专利号:   CN106318276-A
  • 发明人:   SONG Y
  • 专利权人:   QINGDAO SHIKONG MECHANICAL TECHNOLOGY CO
  • 国际专利分类:   C09J011/00, C09J011/06, C09J123/08
  • 专利详细信息:   CN106318276-A 11 Jan 2017 C09J-123/08 201713 Pages: 5 Chinese
  • 申请详细信息:   CN106318276-A CN10403371 11 Jul 2015
  • 优先权号:   CN10403371

▎ 摘  要

NOVELTY - Preparation of anti-aging UV curing adhesive comprises vacuum-drying graphene under nitrogen atmosphere at room temperature for 2-3 hours, adding acetone, stirring for 45-50 minutes, adding 3-5% titanium tetrachloride and magnesium chloride mixture and stirring at 40-60 degrees C for 3-5 hours; ball milling with high purity nitrogen gas and grinding for 5-6 hours; mixing with crosslinking agent TAIC at 30 degrees C; and adding 20-30 wt.% accelerator, wetting agent, dispersing agent and mixed solvent, heating at 165 degrees C for 8-10 minutes and curing under shearing force field for 12-15 minutes. USE - Method for preparing anti-aging UV curing adhesive (claimed). ADVANTAGE - The adhesive has improved bonding strength and peeling strength.