• 专利标题:   Multi-fluorescent nitrogen-doped graphene quantum dots in selective determination of iron ions in solution, prepared by e.g. performing electrolysis, centrifuging the electrolytic solution to obtain solid powder, separating and purifying.
  • 专利号:   CN111269714-A
  • 发明人:   ZHI J, FU Y, GAO G
  • 专利权人:   TECH INST PHYSICS CHEM CHINESE ACAD, UNIV CHINESE ACAD SCI
  • 国际专利分类:   B82Y020/00, B82Y030/00, B82Y040/00, C09K011/65, C25B001/00, G01N021/64
  • 专利详细信息:   CN111269714-A 12 Jun 2020 C09K-011/65 202056 Pages: 9 Chinese
  • 申请详细信息:   CN111269714-A CN11473237 04 Dec 2018
  • 优先权号:   CN11473237

▎ 摘  要

NOVELTY - Multi-fluorescent nitrogen-doped graphene quantum dots, is claimed. The multi-fluorescent nitrogen-doped graphene quantum dots are graphene quantum dots having hydroxy groups and amino groups on the surface obtained by modifying semicarbazide. USE - The multi-fluorescent nitrogen-doped graphene quantum dots are useful in selective determination of iron ions in solution (claimed). ADVANTAGE - The quantum dots: have uniform particle size; and emits blue, green, and red fluorescence in aqueous solution. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are is also included for: (1) preparing multi-fluorescent nitrogen-doped graphene quantum dots, comprising (i) performing electrolysis by taking graphite rods are as cathode and anode, and mixed solution of alkaline aqueous solution and semicarbazide is as electrolyte, and continuing electrolysis until the reaction is full after the surface layer of the graphite rod expands, and (ii) centrifuging the electrolytic solution after electrolysis to obtain solid powder, and separating and purifying the obtained solid powder to obtain multi-fluorescent nitrogen-doped graphene quantum dots; (2) use of multi-fluorescent nitrogen-doped graphene quantum dots in selective determination of iron ions in solution; and (3) use method comprises dissolving multi-fluorescent nitrogen-doped graphene quantum dots in deionized water to prepare aqueous solutions of graphene quantum dots having different concentrations and taking equal volumes of prepared different metal ion solutions having same concentration in the same amount of aqueous solution of graphene quantum dots.