• 专利标题:   Synthesizing beta-tricalcium phosphate nano-material involves dispersing graphene oxide in deionized water to obtain graphene oxide solution, and then adding calcium salt into graphene oxide solution.
  • 专利号:   CN106315534-A
  • 发明人:   WU Q, HAUNG W
  • 专利权人:   UNIV WUHAN TECHNOLOGY
  • 国际专利分类:   C01B025/32
  • 专利详细信息:   CN106315534-A 11 Jan 2017 C01B-025/32 201720 Pages: 9 Chinese
  • 申请详细信息:   CN106315534-A CN10700694 22 Aug 2016
  • 优先权号:   CN10700694

▎ 摘  要

NOVELTY - Synthesizing beta -tricalcium phosphate nano-material involves dispersing graphene oxide in deionized water to obtain graphene oxide solution (0.1-0.8 mg/mL concentration), and adding calcium salt into the graphene oxide solution, and then stirring the mixture to obtain calcium salt solution marked as solution A (0.02344-0.1875mmol/mL concentration). Calcium dihydrogen phosphate and calcium salt are mixed in molar ratio of 2:3, and then ammonium dihydrogen phosphate is added to obtained mixed solution to obtain a solution B, where the pH value is adjusted to 10. USE - Method for synthesizing beta -tricalcium phosphate nano-material (claimed). ADVANTAGE - The method enables to synthesize beta -tricalcium phosphate nano-material in a simple, cost-effective and eco-friendly manner. DETAILED DESCRIPTION - Synthesizing beta -tricalcium phosphate nano-material involves dispersing graphene oxide in deionized water to obtain graphene oxide solution (0.1-0.8 mg/mL concentration), and adding calcium salt into the graphene oxide solution, and then stirring the mixture to obtain calcium salt solution marked as solution A (0.02344-0.1875mmol/mL concentration). Calcium dihydrogen phosphate and calcium salt are mixed in molar ratio of 2:3, and then ammonium dihydrogen phosphate is added to obtained mixed solution to obtain a solution B, where the pH value is adjusted to 10. The solution A and solution B are mixed to obtain solution C. The solution C is centrifugally washed, and then dried to obtain precursor. The precursor is kept in a ceramic crucible, where the ceramic crucible containing precursor is treated in a muffle furnace at 750 degrees C for 1 hour. The obtained product is naturally cooled to room temperature to obtain the finished product i.e. beta -tricalcium phosphate nano-material.