• 专利标题:   Preparing graphene and graphene quantum dot comprises e.g. adding deionized water into a container equipped with a stirring device, adding soluble starch at room temperature or heating stirring and then dispersing.
  • 专利号:   CN108455581-A
  • 发明人:   CHEN W, LV G, HU Y, LI Y, CHEN S, LI D, DAI Z
  • 专利权人:   UNIV CHINA THREE GORGES
  • 国际专利分类:   B82Y020/00, C01B032/184, C09K011/65
  • 专利详细信息:   CN108455581-A 28 Aug 2018 C01B-032/184 201861 Pages: 8 Chinese
  • 申请详细信息:   CN108455581-A CN10301046 04 Apr 2018
  • 优先权号:   CN10301046

▎ 摘  要

NOVELTY - Preparing graphene and graphene quantum dot comprises (i) adding deionized water into a container equipped with a stirring device, adding soluble starch at room temperature or heating at 40-80 degrees C, stirring and dispersing for 10-30 minutes to dissolve (ii) adding solution obtained in step (i) into the hydrothermal kettle at a pressure of 8 Mpa, heating at 120-250 degrees C and carrying out hydrothermal reaction for 1-15 hours to obtain a brown material, and (iii) centrifuging the brown material obtained in step (ii) in a centrifuge at a speed of 3000-15000 revolutions per minute, separating a brown precipitate, lyophilizing to obtain graphene powder and then separating the upper layer of light yellow transparent liquid i.e. an aqueous solution of graphene quantum dots. USE - The method is useful for preparing graphene and graphene quantum dot. ADVANTAGE - The graphene and graphene quantum dot: has excellent fluorescent property.