• 专利标题:   Manufacture of graphene nanowall involves placing quartz boat containing foamed nickel and ferrocene in heating zone at inflow end of purging of reaction gas, heating, purging gas comprising hydrogen and carbon source gas and cooling.
  • 专利号:   CN107619042-A
  • 发明人:   WU F, DAI G, HU H, JIANG B, YAN X, DENG S, ZENG Z
  • 专利权人:   UNIV NANCHANG
  • 国际专利分类:   C01B032/186
  • 专利详细信息:   CN107619042-A 23 Jan 2018 C01B-032/186 201812 Pages: 7 Chinese
  • 申请详细信息:   CN107619042-A CN10927169 09 Oct 2017
  • 优先权号:   CN10927169

▎ 摘  要

NOVELTY - Manufacture of graphene nanowall involves placing a quartz boat containing foamed nickel and ferrocene in a heating zone at inflow end of purging of reaction gas, placing a quartz boat cleaned with stainless steel sheet or wire mesh at heating zone close to reaction gas outflow end, heating to 1000-1200 degrees C under inert gas atmosphere, purging gas comprising hydrogen and carbon source gas in volume ratio of 1:6-2:3, reacting for 1 minute to 3 hours, and cooling to room temperature using inert gas comprising argon or nitrogen. USE - Manufacture of graphene nanowall. ADVANTAGE - The method enables simple and economical large-scale manufacture of thin-transparent graphene nanowall having large surface area and reduced surface defects. DETAILED DESCRIPTION - Manufacture of graphene nanowall involves placing a quartz boat containing foamed nickel and ferrocene in a heating zone at inflow end of purging of reaction gas, placing a quartz boat cleaned with stainless steel sheet or wire mesh at heating zone close to reaction gas outflow end, heating to 1000-1200 degrees C under inert gas atmosphere, purging gas comprising hydrogen and carbon source gas in volume ratio of 1:6-2:3, reacting for 1 minute to 3 hours, and cooling to room temperature using inert gas comprising argon or nitrogen at flow rate of 10-40 sccm. The carbon source gas is hydrocarbon. The flow rate of carbon source gas is 80-180 sccm.