• 专利标题:   Preparation of antistatic modified polybutylene terephthalate fiber by stirring modified graphene, nano metal compound and butylene glycol, adding terephthalic acid and catalyst, heating, reacting, adding antioxidant 1010, and vacuumizing.
  • 专利号:   CN105970340-A, CN105970340-B
  • 发明人:   WU H
  • 专利权人:   YIZHENG SHENGDA NEW TEXTILE MATERIALS CO
  • 国际专利分类:   C08G063/183, D01F001/09, D01F001/10, D01F006/92
  • 专利详细信息:   CN105970340-A 28 Sep 2016 D01F-006/92 201709 Pages: 5 Chinese
  • 申请详细信息:   CN105970340-A CN10482978 27 Jun 2016
  • 优先权号:   CN10482978

▎ 摘  要

NOVELTY - An antistatic modified polybutylene terephthalate fiber is prepared by adding modified graphene, nano metal compound and butylene glycol into reaction kettle, stirring at 50-60 degrees C for 0.5-1 hour, adding terephthalic acid and catalyst, heating at 200-220 degrees C, reacting for 2-3 hours, adding antioxidant 1010 and stabilizer, vacuumizing, heating to 250-280 degrees C, condensing for 3-5 hours to viscosity of 0.6-0.9 to obtain antistatic modified polybutylene terephthalate polyester, melt spinning into screw spinning machine, cooling, oiling, pre-drawing, and rolling, and drawing. USE - Method for preparing antistatic modified polybutylene terephthalate fiber (claimed). ADVANTAGE - The fiber is non-toxic, and has high lasting antistatic property, stable performance and good heat resistance and durability. DETAILED DESCRIPTION - An antistatic modified polybutylene terephthalate fiber is prepared by adding modified graphene, nano metal compound and butylene glycol into reaction kettle, stirring at 50-60 degrees C for 0.5-1 hour, adding terephthalic acid and catalyst, heating at 200-220 degrees C, reacting for 2-3 hours, adding antioxidant 1010 and stabilizer, vacuumizing, heating to 250-280 degrees C, condensing for 3-5 hours to viscosity of 0.6-0.9 to obtain antistatic modified polybutylene terephthalate polyester, melt spinning into screw spinning machine, cooling, oiling, pre-drawing, and rolling, and drawing. The raw material comprises 45-50 pts. wt. terephthalic acid, 34-43 pts. wt. butylene glycol, 0.5-1 pts. wt. catalyst, 8-12 pts. wt. modified graphene, 3-8 pts. wt. nano metal compound, 0.1-0.5 pt. wt. antioxidant 1010, and 0.3-0.8 pt. wt. stabilizer.