• 专利标题:   Silicon oxycarbide composite negative electrode material for lithium ion battery, is prepared by placing wood powder and polysiloxane in furnace, sintering followed by grinding graphene oxide, subjecting thermal reduction and cooling.
  • 专利号:   CN107910554-A
  • 发明人:   PAN J, SHEN W, SHEN X, CHEN B, SUN H, ZHAO Y, YAN X, CHENG X
  • 专利权人:   UNIV JIANGSU
  • 国际专利分类:   H01M010/0525, H01M004/60
  • 专利详细信息:   CN107910554-A 13 Apr 2018 H01M-004/60 201833 Pages: 9 Chinese
  • 申请详细信息:   CN107910554-A CN11011373 26 Oct 2017
  • 优先权号:   CN11011373

▎ 摘  要

NOVELTY - A silicon oxycarbide composite negative electrode material is prepared by placing mixture of wood powder and polysiloxane in a tube furnace and sintering at a high temperature under the protection of argon gas. The temperature is raised to 800-1000 degrees C at a rate of 5 degrees C/minute. The furnace is cooled to obtain silicon oxycarbide ceramic powder. The ceramic powder and the graphene oxide are ground at a certain ratio to obtain a mixture. The mixture is subjected to a thermal reduction under an atmosphere of argon gas, and cooling the furnace. USE - Silicon oxycarbide composite negative electrode material for lithium ion battery. ADVANTAGE - The material has improved conductivity and can effectively improve irreversible capacity loss and voltage hysteresis of the silicon oxycarbide. DETAILED DESCRIPTION - A silicon oxycarbide composite negative electrode material is prepared by placing mixture of wood powder and polysiloxane in a tube furnace and sintering at a high temperature under the protection of argon gas, where the sintering temperature is 50 degrees C, and the temperature is raised to 400 degrees C at a rate of 5 degrees C/minute, and the temperature is maintained for 30 minutes. The temperature is raised to 800-1000 degrees C at a rate of 5 degrees C/minute. The furnace is cooled to obtain silicon oxycarbide ceramic powder. The ceramic powder and the graphene oxide are ground at a certain ratio to obtain a mixture. The mixture is subjected to a thermal reduction under an atmosphere of argon gas, at initial temperature of 50 degrees C, and raising temperature to a suitable temperature at a rate of 5 degrees C/minute and cooling the furnace.