• 专利标题:   Preparing porous graphene lithium-ion battery cathode material comprises preparing graphite oxide modified hummer and preparing porous graphene hydrothermal-solvothermal self-assembly by configuring graphene oxide solution.
  • 专利号:   CN105439128-A
  • 发明人:   CHEN X, HAN Y, LIU H, LIU S, SHENG P, WANG B, XU L, ZHAO G
  • 专利权人:   STATE GRID CORP CHINA, STATE GRID SMART GRID INST, STATE GRID HENAN ELECTRIC POWER CO
  • 国际专利分类:   C01B031/04, H01M010/0525, H01M004/587
  • 专利详细信息:   CN105439128-A 30 Mar 2016 C01B-031/04 201637 Pages: 8 English
  • 申请详细信息:   CN105439128-A CN10759703 09 Nov 2015
  • 优先权号:   CN10759703

▎ 摘  要

NOVELTY - Preparing porous graphene lithium-ion battery cathode material comprises: (i) preparing graphite oxide modified hummer; (ii) preparing porous graphene hydrothermal-solvothermal self-assembly by (ii.a) configuring graphene oxide solution by dispersing the graphite oxide solution under ultrasound; (ii.b) carrying out hydrothermal or solvent thermal reaction of step (ii.a) resultant, (ii.c) displacing organic solvent of step (ii.b) resultant with deionized water and lyophilizing to obtain porous graphene; and (iii) carrying out reduction-doping process of porous graphene into thin film. USE - The lithium-ion battery cathode material is useful in preparing porous graphene (claimed). ADVANTAGE - The cathode material has discharge capacity upto 175 mAh/g with cycle stability. The preparation method is economical and suitable for large-scale industrial production. DETAILED DESCRIPTION - Preparing porous graphene lithium-ion battery cathode material comprises: (i) preparing graphite oxide modified hummer; (ii) preparing porous graphene hydrothermal-solvothermal self-assembly by (ii.a) configuring graphene oxide solution by dispersing the graphite oxide solution under ultrasound for 10minutes- 10 hours; (ii.b) carrying out hydrothermal or solvent thermal reaction of step (ii.a) resultant at 80-240 degrees C for 30 minutes-48 hours, (ii.c) displacing organic solvent of step (ii.b) resultant with deionized water and lyophilizing to obtain porous graphene; and (iii) carrying out reduction-doping process of step (ii) porous graphene into thin film.