• 专利标题:   Preparation of graphene, involves dispersing reaction solution containing to carbonaceous material and potassium permanganate powder, filtering, washing black solid, and subjecting crude graphene to high temperature graphitization.
  • 专利号:   CN106379896-A, CN106379896-B
  • 发明人:   KONG L, SHANG W, YE Y, ZHU X, FANG D
  • 专利权人:   SHENZHEN DYNANONIC CO LTD
  • 国际专利分类:   C01B032/225
  • 专利详细信息:   CN106379896-A 08 Feb 2017 C01B-032/225 201734 Pages: 8 Chinese
  • 申请详细信息:   CN106379896-A CN10854015 27 Sep 2016
  • 优先权号:   CN10854015

▎ 摘  要

NOVELTY - Preparation of graphene, involves adding carbonaceous material to concentrated sulfuric acid, immersing potassium permanganate powder in sulfuric acid, subjecting reaction solution to shear dispersion treatment or ultrasonic treatment to obtain pre-stripped reaction solution, adding deionized water to pre-stripped reaction solution, and filtering, washing resulting solid with hydrochloric acid, and drying, to obtain a black solid, blasting the black solid, to obtain crude graphene, and subjecting crude graphene to high temperature graphitization to obtain purified graphene. USE - Preparation of graphene (claimed). ADVANTAGE - The preparation process is simplified and the production yield is high. The graphene is obtained with complete crystal structure with few layers and excellent conductivity. The production cost is reduced. DETAILED DESCRIPTION - Preparation of graphene, involves adding carbonaceous material to concentrated sulfuric acid, immersing potassium permanganate powder in concentrated sulfuric acid, and stirring the mixture at 20-30 degrees C for 0.5-5 hours, to obtain a reaction solution, subjecting the reaction solution to a shear dispersion treatment or an ultrasonic treatment to obtain a pre-stripped reaction solution, adding deionized water to pre-stripped reaction solution, without stirring, and filtering, washing resulting solid with hydrochloric acid, filtering and drying, to obtain a black solid, blasting the black solid at 300-1200 degrees C for 20-60 seconds, to obtain crude graphene, and subjecting the crude graphene to high temperature graphitization to obtain purified graphene. The carbonaceous material is in the form of a tube or a sheet.