• 专利标题:   Preparation of high-quality graphene used for composite material in enhancing phase or drug carrier with benzene ring comprises putting crude graphite alkene powder into hydrochloric acid solution and performing magnetic force stirring.
  • 专利号:   CN102976320-A
  • 发明人:   OU J, WANG F, JIANG Y
  • 专利权人:   UNIV GUILIN TECHNOLOGY
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102976320-A 20 Mar 2013 C01B-031/04 201369 Pages: 5 Chinese
  • 申请详细信息:   CN102976320-A CN10000094 03 Jan 2013
  • 优先权号:   CN10000094

▎ 摘  要

NOVELTY - A high-quality graphene is prepared by (A) preparing crude graphite alkene powder and magnesium powder; and (B) putting crude graphite alkene powder into 1-10 mol/L hydrochloric acid solution, performing magnetic force stirring for 40-80 minutes to remove unreacted metal magnesium and other soluble impurities, filtering, using deionized water to wash until neutral, placing to obtain black graphene powder at 100-150 degrees C in oven. The step (A) putting metal magnesium powder into tube-type high temperature furnace at flow rate of 50-75 mL/minute under protection of carbon dioxide. USE - Method for preparation of high-quality graphene (claimed) used for composite material in enhancing phase or drug carrier with benzene ring in light, electricity, chemistry and physics. ADVANTAGE - The method is simple, fast, safe and environment-friendly. DETAILED DESCRIPTION - High-quality graphene is prepared by (A) preparing crude graphite alkene powder and magnesium powder; and (B) putting crude graphite alkene powder into 1-10 mol/L hydrochloric acid solution, performing magnetic force stirring for 40-80 minutes to remove unreacted metal magnesium and other soluble impurities, filtering, using deionized water to wash until neutral, placing to obtain black graphene powder at 100-150 degrees C in oven. The step (A) putting metal magnesium powder into tube-type high temperature furnace at flow rate of 50-75 mL/minute under protection of carbon dioxide, and performing magnesium powder combustion at 500-800 degrees C, where flow rate of carbon dioxide is increased to 100-300 mL/minute to meet requirement of burning magnesium powder, and reacting for 20-60 hours at room temperature for directly burning and complete until the magnesium powder burn complete; and under protection of carbon dioxide at flow rate of 70-75 mL/minute, cooling to room temperature, collecting crude graphite alkene powder and magnesium powder. The metal magnesium powder has purity of 90.00-99.99%.