• 专利标题:   Preparation of graphene oxide/rare earth complex luminescent material for production of molecular probes with fluorescent properties, by mixing graphene oxide solution and rare earth/ethanol solution, centrifuging and drying.
  • 专利号:   CN108441210-A
  • 发明人:   HUANG L, CHENG M, TANG J, WANG Y
  • 专利权人:   UNIV QINGDAO
  • 国际专利分类:   C09K011/06, C09K011/02, C09K011/65, G01N021/64, A61K041/00, A61P035/00
  • 专利详细信息:   CN108441210-A 24 Aug 2018 C09K-011/06 201868 Pages: 11 Chinese
  • 申请详细信息:   CN108441210-A CN10348011 18 Apr 2018
  • 优先权号:   CN10348011

▎ 摘  要

NOVELTY - Preparation of graphene oxide/rare earth complex luminescent material involves preparing 1 mg/ml aqueous solution of graphene oxide, ultrasonically dispersing, preparing 0.1 mol/l phenanthroline/ethanol solution, adding 2-50 ml graphene oxide aqueous solution, magnetically stirring to obtain graphene oxide/phenanthroline mixed solution, centrifuging, washing precipitate with anhydrous ethanol 3-4 times, re-dissolving in 50 ml anhydrous ethanol, adding 2 ml rare earth/ethanol solution, magnetically stirring, dripping 0.1 mol/l 2-thiophene trifluoroacetone/ethanol solution, adjusting pH value to 6-7 using aqueous ammonia solution, stirring at 55 plus minus 2 degrees C for 6 plus minus 1 hour, centrifuging, washing separated product 3-4 times with absolute ethanol and drying obtained product in oven at 45 degrees C. USE - Preparation of graphene oxide/rare earth complex luminescent material for production of molecular probes with fluorescent properties and articles having photothermal sensitivity properties (all claimed). ADVANTAGE - The method enables simple preparation of graphene oxide/rare earth complex luminescent material with improved yield, thermal stability and high-temperature resistance, and prolonged fluorescence lifetime.