• 专利标题:   Preparation of magnetic graphene oxide adsorbent for degradation of arsenic, involves ultrasonically processeing graphene oxide, adding trivalent iron salt and ammonia to mixture, concentrating mixture, and calcining dried mixture.
  • 专利号:   CN104772115-A
  • 发明人:   DU C, HAN S, XU J, XU S, YU F, SUN S, SHUI F
  • 专利权人:   SHANGHAI INST TECHNOLOGY
  • 国际专利分类:   B01J020/20, B01J020/30
  • 专利详细信息:   CN104772115-A 15 Jul 2015 B01J-020/20 201607 Pages: 5 Chinese
  • 申请详细信息:   CN104772115-A CN10134709 25 Mar 2015
  • 优先权号:   CN10134709

▎ 摘  要

NOVELTY - 1 g/L Aqueous solution of graphene oxide is ultrasonically processed for 13 hours. A trivalent iron salt is added to mixture and magnetically stirred for 2.5 hours. Excess ammonia is added to mixture, and pH is adjusted to 10.5-11 and maintained for 90 minutes. The mixture is heated, concentrated at 60-70 degrees C to form viscous state, and temperature is controlled to -80 degrees C to -70 degrees C and freeze dried. The dried solids are placed in tube furnace and calcined at 450 degrees C for 2 hours under nitrogen protection, to obtain magnetically oxidized graphene adsorbent. USE - Preparation of magnetic graphene oxide adsorbent (claimed) for degradation of arsenic. ADVANTAGE - The method enables preparation of magnetic graphene oxide adsorbent having excellent physical and chemical properties, arsenic adsorption characteristics and rapid magnetic separation characteristics by economical method.