• 专利标题:   Preparing nano antibacterial stone needle fiber material useful for cotton pad in cosmetics, comprises e.g. adding zinc salt and stone needle to oleylamine, magnetically stirring, introducing inert gas argon, gradually heating, mixing solution to obtain first liquid, injecting ethanol, and stirring.
  • 专利号:   CN113463224-A
  • 发明人:   DAI Y, ZHU J, FANG Z, FANG Y
  • 专利权人:   HEYE HEALTH TECHNOLOGY CO LTD
  • 国际专利分类:   D01D005/00, D01F001/10, D01F009/00
  • 专利详细信息:   CN113463224-A 01 Oct 2021 D01F-009/00 202197 Chinese
  • 申请详细信息:   CN113463224-A CN10746914 02 Jul 2021
  • 优先权号:   CN10746914

▎ 摘  要

NOVELTY - Preparing nano antibacterial stone needle fiber material comprises (1) adding zinc salt and stone needle to oleylamine in mass ratio of 1:4-6, magnetically stirring, introducing the inert gas argon into it for 20-30 minutes, gradually heating the solution to 120-150degreesC, and fully mixing solution to obtain the first liquid; (2) injecting ethanol into above-mentioned first liquid at flow rate of 1-2 ml/min, magnetically stirring for 30-60 minutes under this temperature condition, heating it to 280-300degreesC, keeping the reaction mixture at this temperature for 20-30 minutes, naturally cooling to room temperature to obtain the second liquid; and (3) dropwise adding the second liquid to liquid heptane, centrifuging and separating the precipitate, and drying obtained product in vacuum oven at 60-80degreesC, to obtain the stone needle@zinc oxide nano-sheets. USE - The fiber material is useful for cotton pad in cosmetics and daily chemicals (claimed). ADVANTAGE - The fiber material: has good antibacterial effect, antibacterial rate is greater than 98%; and is simple and easy to prepare. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for the nano antibacterial stone needle fiber material is prepared by above mentioned method.