• 专利标题:   Preparing lubricating additive used in lubricant to prepare cold rolling fluid, by subjecting amino group-containing polyethylene glycol derivative and carboxylated graphene to amidation reaction to form single-ended carboxylated graphene.
  • 专利号:   CN108130159-A
  • 发明人:   WANG Y, HU Y, ZHAO H, ZENG Z, XUE Q
  • 专利权人:   NINGBO INST MATERIALS TECHNOLOGY ENG C
  • 国际专利分类:   C10M159/12, C08G018/66, C08G018/48, C08G018/32, C10M173/02, C10N030/06, C10N040/06, C10N040/08, C10N040/24
  • 专利详细信息:   CN108130159-A 08 Jun 2018 C10M-159/12 201856 Pages: 10 Chinese
  • 申请详细信息:   CN108130159-A CN10046854 18 Jan 2018
  • 优先权号:   CN10046854

▎ 摘  要

NOVELTY - The method for preparing graphene aqueous lubricating additive involves (a) reacting homogeneous mixing system (i) comprising amino protecting group compound and ethanolamine to form amino-protected ethanolamine, (b) reacting a homogeneous mixing system (ii) comprising polyethylene glycol, bridging agent and amino-protected ethanolamine to form amino group-containing polyethylene glycol derivative, and (c) subjecting the amino group-containing polyethylene glycol derivative as modifier and carboxylated graphene to amidation reaction to form a single-ended polyethylene glycol derivative-modified carboxylated graphene with an amino group to obtain graphene aqueous lubricating additive. USE - Method is useful for preparing graphene aqueous lubricating additive, which is useful in aqueous-based lubricant for preparing micro-mechanical lubricating fluid, aqueous hydraulic fluid and cold rolling fluid (all claimed). ADVANTAGE - The method enables simple and energy-efficient preparation of graphene aqueous lubricating additive with excellent wear resistance, safety performance and cooling performance. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) the graphene aqueous lubricating additive prepared by the above method; and (2) aqueous-based lubricant, which comprises 0.005-0.1 wt.% graphene aqueous lubricating additive and water.