• 专利标题:   Preparing graphene oxide modified flame retardant polyol involves adding polyol and flame retardant to the reaction device, and heating catalyst to under alkaline conditions, carrying out reaction for and allowing reaction to cool.
  • 专利号:   CN110183644-A
  • 发明人:   HE J, LI T, LIU T
  • 专利权人:   HUBEI WEIHAN EQUIP TECHNOLOGY CO LTD
  • 国际专利分类:   C08G065/328, C08G065/333, C08G065/335
  • 专利详细信息:   CN110183644-A 30 Aug 2019 C08G-065/328 201974 Pages: 4 Chinese
  • 申请详细信息:   CN110183644-A CN10383435 09 May 2019
  • 优先权号:   CN10383435

▎ 摘  要

NOVELTY - Preparing graphene oxide modified flame retardant polyol involves adding 40-80 pts. wt. polyol and 0.1-30 pts. wt. flame retardant to the reaction device, and heating catalyst to 90-200 degrees C under alkaline conditions, carrying out reaction for 6-12 hours, and allowing reaction to cool to room temperature, using a centrifuge to centrifuge at 300-8000 revolutione per minutes, and removing supernatant to remove catalyst and water molecules. The 0.1-5 pts. wt. graphene oxide and 0.1-2 pts. wt. dispersing agent is added into reaction device, dispersed at high speed for 2-4 h, rotated at 100-500 revolutions per minute, forming a stable phase, and heated to 60-100 degrees C, continuously stirred for 1-65 hours. The temperature inside reaction device is lowered to 20-40 degrees C, unreacted graphene oxide is removed by centrifugation at 5000-10000 revolutions per minutes, and then water is removed by distillation under reduced pressure to obtain a graphene-modified flame retardant polyol. USE - Method for preparing graphene oxide modified flame retardant polyol. ADVANTAGE - The method enables to prepare graphene oxide modified flame retardant polyol that improves flame retardant properties of the polyol to develop a polyol with inflaming retarding effect.