• 专利标题:   Preparation method of macroporous adsorption resin used for polyphenol purification, involves mixing water phase containing water and dispersant and oil phase containing toluene, n-hexane, porogen, initiator and graphene powder, stirring and heating, adding functionalization reagents, washing.
  • 专利号:   CN113713787-A
  • 发明人:   YANG H, YANG Q
  • 专利权人:   BENGBU TIANXING RESIN CO LTD
  • 国际专利分类:   B01D015/08, B01J020/26, B01J020/30
  • 专利详细信息:   CN113713787-A 30 Nov 2021 B01J-020/26 202219 Chinese
  • 申请详细信息:   CN113713787-A CN11196719 14 Oct 2021
  • 优先权号:   CN11196719

▎ 摘  要

NOVELTY - Preparation method of macroporous adsorption resin involves pouring pure water and dispersant into the container and stirring to form the water phase. Mixing toluene, n-hexane, porogen, initiator and graphene powder to form an oil phase. Mixing water phase and oil phase, stirring and heating evenly to obtain copolymerized white spheres, and adding functionalization reagents to the copolymerized white spheres to shape the adsorption resin. Washing the formed adsorbent resin and separating with water. USE - Preparation method of macroporous adsorption resin used for polyphenol purification. ADVANTAGE - Graphene and the anthocyanin are added in the process of manufacturing the adsorption resin, so that the heat resistance and the adsorption effect of the adsorption resin are enhanced, the purification effect of the adsorption resin is better, and meanwhile, the toxic substances in the process of manufacturing the adsorption resin are reduced, so that the adsorption resin is safer to use. Cellulase is added into the adsorption resin, so that the purification efficiency of the adsorption resin on polyphenol is improved, and the use effect of the adsorption resin is better. Heating pipe is arranged on the periphery of the long test tube for heating, so that the adsorption resin is heated more uniformly in the manufacturing process, and the phenomenon that the yield of the adsorption resin is influenced due to nonuniform heating is prevented.