• 专利标题:   Preparation of graphene aerogel noble metal catalyst involves taking porous graphene aperture, adding graphene oxide powder, mixing with pure water, mechanically stirring to obtain oxidized graphene water solution, and reacting.
  • 专利号:   CN107694565-A
  • 发明人:   XIE Y, ZHANG Q, ZHANG H, XU X, LUO G, ZHANG W
  • 专利权人:   SHANGHAI TITAN TECHNOLOGY CO LTD
  • 国际专利分类:   B01D053/62, B01D053/86, B01J023/46, B01J023/50, B01J035/04, B01J035/10, B01J037/10, B01J037/16, B01J037/34
  • 专利详细信息:   CN107694565-A 16 Feb 2018 B01J-023/46 201824 Pages: 9 Chinese
  • 申请详细信息:   CN107694565-A CN11034943 30 Oct 2017
  • 优先权号:   CN11034943

▎ 摘  要

NOVELTY - Preparation of graphene aerogel noble metal catalyst involves taking porous graphene aperture by Hummers method to prepare graphene oxide powder; adding graphene oxide powder, mixing with pure water by ultrasonic dispersion, and mechanically stirring to obtain 4-8 mg/mL oxidized graphene water solution; mixing graphene oxide liquid oxidized graphene water solution with noble metal salt, preserving temperature, and reacting; mixing mixed solution into reducing agent L-ascorbic acid, stirring, and carrying out hydrothermal reaction to obtain noble metal graphene hydrogel; and freezing. USE - Method for preparing graphene aerogel noble metal catalyst. ADVANTAGE - The method has simple preparation technique, and good economic benefit. DETAILED DESCRIPTION - Preparation of graphene aerogel noble metal catalyst comprises taking porous graphene aperture by Hummers method to prepare graphene oxide powder; adding graphene oxide powder, mixing with pure water by ultrasonic dispersion, and mechanically stirring to obtain 4-8 mg/mL oxidized graphene water solution; mixing graphene oxide liquid oxidized graphene water solution with noble metal salt, preserving temperature, and reacting; mixing mixed solution into reducing agent L-ascorbic acid, stirring, and carrying out hydrothermal reaction to obtain noble metal graphene hydrogel; and freezing, and drying to remove solvent.