• 专利标题:   Preparation of graphene used for preparation of graphene oxide composite, involves dissolving catechol or catechol derivative in solvent, adding graphene oxide, dispersing, reacting, filtering, washing with water and drying.
  • 专利号:   CN103332678-A, CN103332678-B
  • 发明人:   SHI L, XU H, ZHANG M, WANG Z, YUAN S, ZHAO Y
  • 专利权人:   UNIV SHANGHAI DONGGUAN NANOTECHNOLOGY, UNIV SHANGHAI
  • 国际专利分类:   C01B031/04, C01B033/12, C01G019/02, C01G023/053, C01G025/02, C01G045/02, C01G051/04, C01G053/04
  • 专利详细信息:   CN103332678-A 02 Oct 2013 C01B-031/04 201403 Pages: 10 Chinese
  • 申请详细信息:   CN103332678-A CN10199745 24 May 2013
  • 优先权号:   CN10199745

▎ 摘  要

NOVELTY - Preparation of graphene involves dissolving catechol or catechol derivative in solvent, obtaining 0.05 g/ml solution of catechol or catechol derivative, adding graphene oxide, ultrasonically dispersing for 0.5-4 hours, obtaining dispersion, transferring the obtained dispersion into an autoclave, placing the obtained autoclave into a reactor, reacting at 80-200 degrees C for 12-48 hours under hot water bath, filtering the resultant reaction mixture, washing with water, and drying under vacuum. USE - Preparation of graphene used for preparation of graphene/oxide composite for lithium-ion battery, supercapacitor and electrochemical sensor (claimed). ADVANTAGE - The method provides graphene having excellent disperability, by a simple and environmentally-friendly process. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for use of graphene to prepare a graphene/oxide composite.