• 专利标题:   Using graphene oxide-silicon dioxide composite nucleating additive to improve crystalline property polyester polyester, comprises e.g. taking graphene oxide nanosheet to dissolve in deionized water ultrasonic dispersion.
  • 专利号:   CN114318577-A
  • 发明人:   LIU Z, SHEN W, WANG W, HUANG L, LIU J, TANG J, HAO T, WANG Y
  • 专利权人:   UNIV QINGDAO
  • 国际专利分类:   D01F001/10, D01F006/92
  • 专利详细信息:   CN114318577-A 12 Apr 2022 D01F-006/92 202257 Chinese
  • 申请详细信息:   CN114318577-A CN10161012 22 Feb 2022
  • 优先权号:   CN10161012

▎ 摘  要

NOVELTY - Preparing graphene and silica composite material comprises dissolving 20-9.5 ml graphene oxide-silicate (GO-SiO2) in deionized water, ultrasonically crushing and dispersing; adding 1 ml polyethylene terephthalate (IPTES) with formic acid to adjust pH to 4-5, refluxing at 70degrees Celsius for 6 hours; using ethanol to wash for 2-3 times to obtain GO-SiO2-IPTETES, dispersing 10 g of GO-SiO2 -ipTES in 10 g dimethylformamide (DMF); dispersing 50 mg LMPET-PEG dispersed in 5.5 ml DMF; mixing two components; and adding 50 mg dibutyl tin laurate (DBDU) and heating. USE - The method is useful for improving crystal performance of polyester fiber, preferably polyethylene glycol terephthalate (PET). ADVANTAGE - The method increases the compatibility of the additive and PET by grafting block, polymer to the PET for spinning increases the crystallization performance and thermal performance of the PET fiber. The modified PET fiber has good thermodynamic stability, good crystallization and very good application prospect. DESCRIPTION OF DRAWING(S) - The drawing shows a SEM image of PET fiber by the method.