• 专利标题:   Preparing single-walled carbon nano-tube useful for preparing field-effect transistor device, comprises e.g. ultrasonically cleaning growth substrate, blow-drying, annealing, stripping graphene, and performing chemical vapor deposition.
  • 专利号:   CN113213454-A, CN113213454-B
  • 发明人:   HU Y, ZHANG H, QIAN J, HUANG S
  • 专利权人:   UNIV WENZHOU
  • 国际专利分类:   C01B032/159, C01B032/162, C01B032/19
  • 专利详细信息:   CN113213454-A 06 Aug 2021 C01B-032/162 202172 Pages: 15 Chinese
  • 申请详细信息:   CN113213454-A CN10430294 21 Apr 2021
  • 优先权号:   CN10430294

▎ 摘  要

NOVELTY - Preparing single-walled carbon nano-tube comprises: (i) orderly and ultrasonically cleaning growth substrate in ultra-pure water, acetone, ethanol and ultra-pure water, blow-drying by using high-purity nitrogen, placing cleaned substrate into muffle furnace, heating to 900 degrees C for 2 hours, annealing in air at 900 degrees C for 8 hours, cooling to 300 degrees C for 10 hours, cooling to room temperature; (ii) mechanically stripping catalyst i.e. graphene on processed growth substrate, where layer number is 1-10 layer; (iii) growing carbon nano-tube on substrate deposited with graphene, and introducing hydrogen and carbon source into chemical vapor deposition system for growth of single-walled carbon nano-tube; and (iv) obtaining full-carbon heterojunction finished product. USE - The method is useful for preparing single-walled carbon nano-tube, which is useful for preparing field-effect transistor device with stable performance. ADVANTAGE - The single-walled carbon nano-tube process does not contain metal.