• 专利标题:   Production of graphite oxide for e.g. manufacture of graphene, involves oxidizing carbon source by reacting e.g. alkali metal ion containing sodium hydroxide, and oxidant containing perchloric acid, adding hydrogen peroxide, and washing.
  • 专利号:   WO2020009421-A1, KR2020004126-A, KR2072914-B1
  • 发明人:   LEE J H, PARK O K, KIM N H, KIM N
  • 专利权人:   UNIV CHONBUK NAT IND COOP FOUND
  • 国际专利分类:   C01B032/192, C01B032/23
  • 专利详细信息:   WO2020009421-A1 09 Jan 2020 C01B-032/23 202008 Pages: 24
  • 申请详细信息:   WO2020009421-A1 WOKR008034 02 Jul 2019
  • 优先权号:   KR077191

▎ 摘  要

NOVELTY - Production of graphite oxide involves chemically oxidizing the carbon source by reacting an alkali metal ion, an oxidant and a carbon source in distilled water or a hydrophilic organic solvent, adding hydrogen peroxide to the oxidized reactant and stirring to terminate the reaction, and washing the reactant from which the reaction is terminated to produce graphite oxide. The alkali metal ion is at least one chosen from sodium hydroxide, potassium hydroxide and bromine hydroxide. The oxidizing agent is at least one chosen from osmium tetroxide, potassium permanganate, potassium chlorate, perchloric acid and hydrogen peroxide. USE - Production of graphite oxide in manufacture of graphene (claimed) used for high-performance polymer composite materials for electrical and electronic devices. ADVANTAGE - The method enables efficient and economical production of graphene oxide having increased conductivity, improved rate of formation, and reduced production time. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for manufacture of graphene, which involves (I) adding graphite oxide onto an organic solvent or distilled water, (II) exfoliating graphite oxide in the organic solvent or distilled water through shear stress or ultrasonically dispersing to produce graphene oxide, and (III) preparing graphene by adding a reducing agent to the graphene oxide.