• 专利标题:   Preparation of iron(III) oxide/reduced graphene oxide composite material used as cathode material for lithium battery, involves reacting solution containing iron sulfate heptahydrate and solution containing graphene oxide and washing.
  • 专利号:   CN104124442-A, CN104124442-B
  • 发明人:   CHEN X, ZHANG F
  • 专利权人:   CHEN X, HAIMEN FENGLONG STAINLESS STEEL PHARM
  • 国际专利分类:   B82Y030/00, B82Y040/00, H01M010/0525, H01M004/36, H01M004/52
  • 专利详细信息:   CN104124442-A 29 Oct 2014 H01M-004/36 201504 Pages: 7 Chinese
  • 申请详细信息:   CN104124442-A CN10311647 02 Jul 2014
  • 优先权号:   CN10311647

▎ 摘  要

NOVELTY - Preparation of iron(III) oxide/reduced graphene oxide composite material involves uniformly mixing solution (A) and solution (B), stirring uniformly, obtaining mixed solution, adding the obtained mixed solution into a reactor, reacting at 140-180 degrees C for 8-12 hours, washing the resultant reaction product using anhydrous ethanol and water and drying under vacuum. The solution (A) is prepared by dissolving iron sulfate heptahydrate in mixture of water and glycerol. The solution (B) is prepared by dispersing graphene oxide in water and ultrasonically dispersing the resultant solution. USE - Preparation of iron(III) oxide/reduced graphene oxide composite material used as cathode material for lithium battery (claimed). ADVANTAGE - The method provides iron(III) oxide/reduced graphene oxide composite material with high quality and stability, by economical and simple process. DETAILED DESCRIPTION - Preparation of iron(III) oxide/reduced graphene oxide composite material involves uniformly mixing solution (A) and solution (B), stirring uniformly, obtaining mixed solution, adding the obtained mixed solution into a reactor, reacting at 140-180 degrees C for 8-12 hours, washing the resultant reaction product using anhydrous ethanol and water several times and drying in an oven at 60-100 degrees C under vacuum. The solution (A) is prepared by dissolving iron sulfate heptahydrate in mixture of water and glycerol. The solution (B) is prepared by dispersing graphene oxide in water and ultrasonically dispersing the resultant solution.