• 专利标题:   Preparation of graphene involves assembling pole piece, counter electrode pole piece, electrolyte containing propylene carbonate, and diaphragm into battery, subjecting battery into charge-discharge test, and stripping graphite layers.
  • 专利号:   CN102530930-A, CN102530930-B
  • 发明人:   HE L, LIU D, WANG Y, XU R, SUN F, YAN X
  • 专利权人:   DONGGUAN AMPEREX TECHNOLOGY CO LTD, NINGDE AMPEREX TECHNOLOGY CO LTD
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102530930-A 04 Jul 2012 C01B-031/04 201303 Pages: 9 Chinese
  • 申请详细信息:   CN102530930-A CN10269176 05 Sep 2011
  • 优先权号:   CN10269176

▎ 摘  要

NOVELTY - Preparation of graphene comprises assembling pole piece containing graphite material, counter electrode pole piece containing lithium, electrolyte containing propylene carbonate, and diaphragm into battery; subjecting battery into charge-discharge test; stripping graphite layers; subjecting battery into charge-discharge test; removing lithium in graphite pole piece; taking apart battery; soaking graphite pole piece into dimethyl carbonate solution; removing impurities on graphite pole piece; washing product with diluted hydrochloric acid; and drying in oven. USE - Preparation of graphene. ADVANTAGE - The method does not use expensive device, has simple operation, provides graphene through simple charge-discharge and post processing, safe and reliable, and has lower cost. DETAILED DESCRIPTION - Preparation of graphene comprises assembling pole piece containing graphite material, counter electrode pole piece containing lithium, electrolyte containing propylene carbonate (PC), and diaphragm into battery; subjecting battery into charge-discharge test; making lithium and PC in counter electrode pole piece form solvent lithium ion and enter graphite layers; stripping graphite layers one by one to form graphene material and lithium carbonate; subjecting battery into charge-discharge test; removing lithium in graphite pole piece; taking apart battery; soaking graphite pole piece into dimethyl carbonate (DMC) solution; removing impurities on graphite pole piece; washing product with diluted hydrochloric acid for several times to remove lithium carbonate; and drying in oven to obtain final product. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic diagram of a process for preparation of graphene (Drawing includes non-English language text).