• 专利标题:   Graphene material useful in e.g. fuel cell oxygen reduction reaction non-noble metal catalyst, super capacitor, comprises e.g. potassium hydroxide, terephthalaldehyde, green alum, graphite, sodium dodecyl sulfate, and magnesium chloride.
  • 专利号:   CN106185889-A
  • 发明人:   DAI X
  • 专利权人:   SUZHOU YUNSHU NEW MATERIAL TECHNOLOGY CO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN106185889-A 07 Dec 2016 C01B-031/04 201712 Pages: 6 Chinese
  • 申请详细信息:   CN106185889-A CN10514928 04 Jul 2016
  • 优先权号:   CN10514928

▎ 摘  要

NOVELTY - Graphene material comprises 100 pts. wt. potassium hydroxide, 5-15 pts. wt. terephthalaldehyde, 4-8 pts. wt. green alum, 2-8 pts. wt. graphite, 1-3 pts. wt. sodium dodecyl sulfate, 4-6 pts. wt. magnesium chloride, 10-12 pts. wt. ethylene glycol monobutyl ether, 3-7 pts. wt. calcium chloride, 6-10 pts. wt. tetramethylammonium bicarbonate, and 7-9 pts. wt. nickel bromide. USE - The graphene material is useful in fuel cell oxygen reduction reaction non-noble metal catalyst, super capacitor, lithium-ion batteries and other energy storage areas and industrial catalysis. ADVANTAGE - The graphene material has mechanical property, conductive property, good thermal conductivity; and is economical, operation is simple and easy, improves battery's high-current discharge property, environmentally friendly, suitable for large-scale production, and has high-current products discharge cycle performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing graphene material comprising (i) taking potassium hydroxide, terephthalaldehyde, green alum, graphite, sodium dodecyl sulfate, magnesium chloride, ethylene glycol monobutyl ether, calcium chloride, tetramethylammonium bicarbonate, and nickel bromide; (ii) transferring feedstock raw material into a mill, grinding at room temperature for 50-60 minutes, to obtain mixture; and (iii) placing the homogenized material in capped ceramic crucible, palcing the ceramic crucible into tube furnace using lid under high-purity nitrogen protection, heating at 550-650 degrees C for 1-5 hours, increasing the heating temperature to 800-1000 degrees C for 2-4 hours, to obtain graphene material.