• 专利标题:   Preparing industrial graphene oxide involves mixing concentrated sulfuric acid with flake graphite, heating to react to obtain acidic mixture, cooling, then adding potassium permanganate and pure water to react, and adding hydrogen peroxide.
  • 专利号:   CN107055525-A
  • 发明人:   CAI Q, REN W, ZHANG Y, YU Y
  • 专利权人:   SHANDONG HAIMAI NEW MATERIALS CO LTD
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN107055525-A 18 Aug 2017 C01B-032/198 201767 Pages: 6 Chinese
  • 申请详细信息:   CN107055525-A CN10450407 15 Jun 2017
  • 优先权号:   CN10450407

▎ 摘  要

NOVELTY - Preparing industrial graphene oxide involves mixing the concentrated sulfuric acid with flake graphite, heating to react to obtain the acidic mixture, cooling the acidic mixture material, adding potassium permanganate and pure water to react, and after finishing reaction, adding hydrogen peroxide to obtain the graphite oxide solution. The product is centrifuged and washed to neutral. The obtained solution is formulated as suspension which is ultrasonically treated and freeze-dried to obtain the graphene oxide. USE - Method for preparing industrial graphene oxide (claimed). ADVANTAGE - The method enables to prepare industrial graphene oxide which has large specific surface area, stable layer number and easy centrifugation.