• 专利标题:   Preparing multifunctional epoxy resin-based water-soluble sizing agent containing graphene oxide comprises e.g. reacting polyfunctional epoxy resin, amino compound containing alcoholic hydroxy group and diluent and stirring.
  • 专利号:   CN107385921-A
  • 发明人:   DAI S, HAO S, REN Z, XING Y, YANG C
  • 专利权人:   AECC BEIJING AERONAUTICAL MATERIALS INST
  • 国际专利分类:   C08G059/32, C08G059/50, D06M101/40, D06M011/74, D06M013/152, D06M013/368, D06M015/03, D06M015/55
  • 专利详细信息:   CN107385921-A 24 Nov 2017 D06M-015/55 201807 Pages: 7 Chinese
  • 申请详细信息:   CN107385921-A CN10565366 12 Jul 2017
  • 优先权号:   CN10565366

▎ 摘  要

NOVELTY - Preparing multifunctional epoxy resin-based water-soluble sizing agent containing graphene oxide comprises (i) reacting polyfunctional epoxy resin, amino compound containing alcoholic hydroxy group and diluent at 60-90 degrees C for 40-150 minutes, then lowering reaction temperature to 45-65 degrees C and adding carboxylic acid compound to continue reaction for 30-60 minutes to obtain water-soluble multi-functional epoxy resin, and (ii) mixing water-soluble polyfunctional epoxy resin and graphene oxide aqueous solution containing bionic compound, and stirring mixed solution at 0-30 degrees C. USE - The method is useful for preparing multifunctional epoxy resin-based water-soluble sizing agent containing graphene oxide (claimed). ADVANTAGE - The sizing agent has high cross-linking density, high glass transition temperature, excellent heat resistance and thermal stability, simple preparation process; and has improved processability inlcuding cluster property and abrasion resistance.