• 专利标题:   Manufacture of radial porous graphene composite beads used for adsorbing e.g. diazepam, involves dispersing graphene oxide in polymer solution, adding suspension into cryogenic freezing bath, freeze-drying beads, crosslinking and reducing.
  • 专利号:   CN107297198-A
  • 发明人:   BAI J, GAN J, GONG Q, HUANG Y, LIANG J, LIU D, SAKAMIYA M
  • 专利权人:   BEIJING HUAQINGTIANXING TECHNOLOGY DEV, UNIV TSINGHUA
  • 国际专利分类:   B01J020/24, B01J020/26, B01J020/28, B01J020/30
  • 专利详细信息:   CN107297198-A 27 Oct 2017 B01J-020/24 201803 Pages: 10 Chinese
  • 申请详细信息:   CN107297198-A CN10369040 23 May 2017
  • 优先权号:   CN10369040

▎ 摘  要

NOVELTY - Manufacture of radial porous graphene composite beads involves uniformly dispersing graphene oxide in a polymer solution to obtain a graphene oxide suspension, adding the graphene oxide suspension into a receiving liquid in a cryogenic freezing bath to obtain crystalline composite beads, freeze-drying the crystalline composite beads to obtain graphene oxide/polymer composite beads, crosslinking the composite beads using a crosslinking agent solution, and reducing the composite beads using a liquid phase or a vapor phase reducing agent. USE - Manufacture of radial porous graphene composite beads used for adsorbing diazepam, vitamin B12, beta 2-microglobulin, interleukin, tumor necrosis factor, parathyroid hormone and hepatitis B virus (all claimed) and used as adsorbent in hemoperfusion therapy. ADVANTAGE - The graphene composite beads have excellent mechanical strength and adsorption characteristics. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for usage of the graphene composite beads in adsorption of diazepam, vitamin B12, beta 2-microglobulin, interleukin, tumor necrosis factor, parathyroid hormone and hepatitis B virus.