• 专利标题:   Preparing mesoporous multilayer graphene, comprises dissolving carbon source and metal catalyst in water, adding nitric acid to it, heating solution to evaporation, so that a fluffy mass is formed, and subjecting fluffy mass to annealing.
  • 专利号:   IN201500990-I2
  • 发明人:   BISWAS S, PANCHANAN P, RAJIB B
  • 专利权人:   BISWAS S, PANCHANAN P, RAJIB B
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   IN201500990-I2 08 Dec 2017 C01B-031/04 201802 Pages: 15 English
  • 申请详细信息:   IN201500990-I2 INKO00990 16 Nov 2015
  • 优先权号:   INKO00990

▎ 摘  要

NOVELTY - Preparing mesoporous multilayer graphene, comprises: dissolving a carbon source and a metal catalyst in water; adding nitric acid to it, to bring the pH to 1; heating the obtained solution to evaporation, so that a fluffy mass is formed; and subjecting the fluffy mass to annealing at a temperature of 700-1000 degrees C to obtain graphene, which is powdered and dried. USE - The process is useful for preparing mesoporous multilayer graphene. ADVANTAGE - The process: provides mesoporous multilayer graphene with surface area of 320 m2/g and narrow pore diameter of 0.37-7 (preferably 3.14) nm (claimed); is fast, cost-effective, environment friendly and suitable for large-scale production of graphene; and utilizes the low cost and non-toxic easily available precursor materials. The graphene layers can be controlled to a minimum of 8 layers. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for the mesoporous multilayer graphene having its surface area of 320 m2/g and narrow pore diameter distribution of 0.37-7 (preferably 3.14) nm, a layer having a thickness of 2-14 nm.