• 专利标题:   Preparing solid film lubricant by bonding method comprises e.g. mixing 4,4'-diaminodiphenyl ether, graphene oxide, 3,3',4,4'-biphenyltetracarboxylic dianhydride, molybdenum disulfide dispersion and then ultrasonically oscillating.
  • 专利号:   CN108251195-A
  • 发明人:   YU Y, XU Y, HUANG H
  • 专利权人:   ZHAO J
  • 国际专利分类:   C10M169/04, C10M177/00, C10N030/06, C10N030/08, C10N050/08
  • 专利详细信息:   CN108251195-A 06 Jul 2018 C10M-169/04 201851 Pages: 7 Chinese
  • 申请详细信息:   CN108251195-A CN11468268 29 Dec 2017
  • 优先权号:   CN11468268

▎ 摘  要

NOVELTY - Preparing solid film lubricant by bonding method comprises (i) mixing 80-100 pts. wt. 4,4'-diaminodiphenyl ether, 6-8 pts. wt. graphene oxide, 10-12 pts. wt. 3,3',4,4'-biphenyltetracarboxylic dianhydride, 10-20 pts. wt. molybdenum disulfide dispersion, 3-5 pts. wt. acetic anhydride and 4-6 pts. wt. pyridine, ultrasonically oscillating, adding 3,3',4,4'-biphenyltetracarboxylic dianhydride and molybdenum disulfide dispersion, continuing ultrasonic oscillation, adding acetic anhydride and pyridine, stirring the reaction, aging to obtain aging gel, and (ii) mixing aging gel and epoxy resin dilution solution in a mass ratio of 1:1-1:3, ultrasonically oscillating, concentrating under reduced pressure, cooling and then filling to obtain final product. USE - The method is useful for preparing solid film lubricant by bonding method. ADVANTAGE - The solid film lubricant: has excellent heat resistance and adhesion ability; and improve the service life of the product.