• 专利标题:   Preparing foam microporous material involves mixing aqueous phase prepared using surfactant and foam stabilizer, and oil phase prepared using chemical monomer and initiator, emulsifying to obtain water in oil type pre-emulsion, passing through microporous membrane to obtain emulsion, and curing.
  • 专利号:   CN113736126-A, CN113736126-B
  • 发明人:   YU B, XU L, SUN H
  • 专利权人:   UNIV ZHEJIANG SCITECH
  • 国际专利分类:   C08F112/08, C08F112/12, C08F120/18, C08F004/38, C08J009/00, C08K005/42, C08L025/06, C08L025/16, C08L033/08, C08L071/02, C08L083/12
  • 专利详细信息:   CN113736126-A 03 Dec 2021 C08J-009/00 202227 Chinese
  • 申请详细信息:   CN113736126-A CN11043041 07 Sep 2021
  • 优先权号:   CN11043041

▎ 摘  要

NOVELTY - Preparing foam microporous material involves: (S1) adding 2-6 pts. wt. surfactant and 1-3 pts. wt. foam stabilizer to 5-10 pts. wt. deionized water to prepare a homogeneous aqueous solution as an aqueous phase, mixing 20-30 pts. wt. chemical monomer, 4-8 pts. wt. initiator and 40-60 pts. wt. N-methylpyrrolidone to obtain a homogeneous oil solution as an oil phase, quickly mixing the aqueous phase and the oil phase, and then preparing water in oil (W/O) type pre-emulsion by homogenizing, emulsifying, stirring or ultrasonic method; (S2) quickly passing the pre-emulsion through a pore size of a microporous membrane under a pressure of 0.5-2 MPa to obtain a W/O-type emulsion with a uniform particle size; and (S3) curing, filtering, washing, and drying the prepared W/O emulsion. USE - The method is useful for preparing foam microporous material. ADVANTAGE - The method provides foam microporous material, which has controllable average particle size and regular cell structure.