• 专利标题:   Preparing vanadium-tungsten double-metal selenide material, comprises adding metal salt and oxidation graphene deionized water, ultrasonically dissolving, adding melamine into deionized water, adding formaldehyde solution, filtering, washing, freezing and carrying out selenizing annealing treatment.
  • 专利号:   CN115535973-A, CN115535973-B
  • 发明人:   YUAN X, DENG Q, WAN Q, CHEN J, SONG Y, WEI X, CHEN Q
  • 专利权人:   SICHUAN SHUWANG NEW ENERGY CO LTD
  • 国际专利分类:   C01B019/00, H01M004/38, H01M004/58
  • 专利详细信息:   CN115535973-A 30 Dec 2022 C01B-019/00 202313 Chinese
  • 申请详细信息:   CN115535973-A CN11332919 28 Oct 2022
  • 优先权号:   CN11332919

▎ 摘  要

NOVELTY - Preparing vanadium-tungsten double-metal selenide material, comprises (i) adding the metal salt and the oxidation graphene deionized water, ultrasonically dissolving for 0.5-1 hour at 10-50℃ to obtain the product A, (ii) adding the melamine into the deionized water, placing into the oil bath pot and stirring to 60-80℃, adding formaldehyde solution to obtain the product B, and (iii) adding the product A into the product B, stirring for 12-24 hours at 10-50℃, filtering, washing, freezing and drying to obtain the graphene tungsten salt precursor of graphite alkenyl, and carrying out selenizing annealing treatment under the inert gas. USE - Preparing vanadium-tungsten double-metal selenide material for sodium ion battery used as rechargeable secondary battery for storing new energy e.g. solar energy, wind energy and hydrogen energy. ADVANTAGE - The method enables to prepare vanadium-tungsten double-metal selenide material, which provides rich active sites for reaction. The built-in electric field formed in the interface effectively enhances the dynamic performance of the battery, and exhibits a higher capacity and excellent multiplying power performance, and has potential in the sodium storage performance.