• 专利标题:   Preparing molybdenum disulfide nano/graphene heterostructure used in fields of semiconductor electronic devices, sensors and catalysis, involves analyzing pure level of molybdate, taking thiourea and ethanol dispersion of graphene.
  • 专利号:   CN107010671-A
  • 发明人:   YANG X, CHAI J, ZHANG D, GU Y, CAO M
  • 专利权人:   UNIV QIQIHAR
  • 国际专利分类:   B82Y030/00, C01B032/194, C01G039/06
  • 专利详细信息:   CN107010671-A 04 Aug 2017 C01G-039/06 201763 Pages: 6 Chinese
  • 申请详细信息:   CN107010671-A CN10207274 31 Mar 2017
  • 优先权号:   CN10207274

▎ 摘  要

NOVELTY - Preparing molybdenum disulfide nano/graphene heterostructure involves analyzing pure level of molybdate, taking thiourea and ethanol dispersion of graphene as raw material, where the molar ratio of ammonium molybdate and thiourea is 1:4, and mixing by using magnetic stirring hydrothermal reaction device. The ammonium molybdate and thiourea are dissolved in de-ionized water, a certain amount of ethanol graphene dispersion is added, magnetically stirred at 200 degrees C for 10 hours to obtain the hydrothermal product. The product is washed with water and alcohol and dried in vacuum. USE - Method fro preparing molybdenum disulfide nano/graphene heterostructure used in fields of semiconductor electronic devices, sensors and catalysis (claimed). ADVANTAGE - The method enables to prepare molybdenum disulfide nano/graphene heterostructure which is easy to process in a simple and controllable manner. It has good performance and wide application prospect. DETAILED DESCRIPTION - Preparing molybdenum disulfide nano/graphene heterostructure involves analyzing pure level of molybdate, taking thiourea and ethanol dispersion of graphene as raw material, where the molar ratio of ammonium molybdate and thiourea is 1:4, and mixing by using magnetic stirring hydrothermal reaction device. The ammonium molybdate and thiourea are dissolved in de-ionized water, a certain amount of ethanol graphene dispersion is added, magnetically stirred at 200 degrees C for 10 hours to obtain the hydrothermal product. The product is washed with water and alcohol and dried in vacuum to obtain the black solid molybdenum disulfide nano graphene/heterostructure.