▎ 摘 要
NOVELTY - Preparing microwave medium glaze water comprises e.g. (1) preparing materials, taking 55.17 wt.% barium carbonate, 25.46 wt.% barium oxide, 4.25 wt.% cobalt oxide, 2.12 wt.% zinc oxide, 0.17 wt.% gallium oxide, 4.81 wt.% graphene oxide, 2.83 wt.% magnesium oxide, and 5.19 wt.% zirconium tungstate, and removing the impurities from the above raw materials; (2) taking barium carbonate, niobium oxide, cobalt oxide, zinc oxide and magnesium oxide corresponding weight according to materials proportion, mixing, using the ball mill to grind for 8-10 hours, then placing into the kiln furnace melting block, insulating for 2 hours, then quenching, water quenching and grinding, (3) taking raw materials of gallium oxide and grinding, adding frit powder into suitable container, adding gallium oxide powder and mixing uniformly, adding water to dilute to prepare glaze slurry; and (4) dispersion of graphene oxide, adding macromolecule dispersant, mixing and performing ultrasonic oscillation. USE - The method is useful for preparing microwave medium glaze water. ADVANTAGE - The method: can improve the final quality of glaze has very important effect, improves the quantity of ceramic products, and has the characteristic of low expansion, and has important industrial use value. DETAILED DESCRIPTION - Preparing microwave medium glaze water comprises (1) preparing materials, taking 55.17 wt.% barium carbonate, 25.46 wt.% barium oxide, 4.25 wt.% cobalt oxide, 2.12 wt.% zinc oxide, 0.17 wt.% gallium oxide, 4.81 wt.% graphene oxide, 2.83 wt.% magnesium oxide, and 5.19 wt.% zirconium tungstate, and removing the impurities from the above raw materials; (2) taking barium carbonate, niobium oxide, cobalt oxide, zinc oxide and magnesium oxide corresponding weight according to materials proportion, mixing, using the ball mill to grind for 8-10 hours, then placing into the kiln furnace melting block, insulating for 2 hours, then quenching, water quenching and grinding, (3) taking raw materials of gallium oxide and grinding, adding frit powder into suitable container, adding gallium oxide powder and mixing uniformly, adding water to dilute to prepare glaze slurry; (4) dispersion of graphene oxide prepared according to the raw material proportion taking suitable amount of graphene oxide powder, placing in a suitable container, adding macromolecule dispersant, mixing them uniformly and performing ultrasonic oscillation for 12 hours, (5) slowly adding zirconium and tungsten-containing solution (0.5 mol/l) to water at room temperature and stirring, the ratio of water, zirconium-containing solution and tungsten-containing solution is 0.25:0.5:1, stirring for 10 hours, then adding hydrochloric acid whose concentration is 6 mol/l, fractionating the mixture for 2 days, after the fractionation for 3 week to make it gelatinized, then pouring out the supernatant, after filtering and washing under 353 K drying in an oven, then heating to 873K for 10 hours, and grinding, (6) adding a suitable amount of zirconium tungstate powder according to the ratio of raw materials to the graphene oxide dispersion in the fourth step and mixing uniformly, and thoroughly irradiating the mixture with far infrared rays for 24 hours to reduce the graphene oxide, and fully combining with zirconium tungstate powder; (7) mixing the glaze slurry obtained in the step (4), and the mixed liquid obtained in the step (6), to form the glaze water, and adjusting the water content of the glaze water to 28-32%; (8) detecting the pH of the glaze water to prepare suitably adjusting; and (9) static-placing the glaze for a specific period of time.