• 专利标题:   Preparation of graphene oxide used for e.g. energy storage, comprises plasma sputtering graphite to obtain modified graphite, adding potassium permanganate to concentrated sulfuric acid to mix uniformly, adding graphite to obtained mixture, and reacting mixture.
  • 专利号:   CN114348998-A
  • 发明人:   ZHU Y, FENG J, GU L
  • 专利权人:   WUXI QIHAO ENVIRONMENTAL PROTECTION NEW MATERIAL RES CO LTD
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN114348998-A 15 Apr 2022 C01B-032/198 202255 Chinese
  • 申请详细信息:   CN114348998-A CN11535865 15 Dec 2021
  • 优先权号:   CN11535865

▎ 摘  要

NOVELTY - Preparation of graphene oxide comprises plasma sputtering graphite to obtain modified graphite; adding potassium permanganate to concentrated sulfuric acid and mixing uniformly to obtain mixture A; adding modified graphite to mixture A to obtain mixture B; reacting mixture B at 25-60degrees Celsius for 2-6 hours to obtain mixture C; adding mixture C into ice water, adding hydrogen peroxide and mixing uniformly; and washing precipitate with water until neutral. USE - The method is for preparing graphene oxide for catalysis, energy storage, heat conduction, and metal corrosion protection. ADVANTAGE - The method provides graphene oxide with high yield, low cost, small danger, fast and simple reaction process, which is very suitable for large-scale industrial production.