• 专利标题:   Self-assembled laminated infrared film material is obtained by laminating layered double hydroxide nanosheet and single layer of graphene oxide alternately, and has thickness of specified range.
  • 专利号:   CN102876287-A, CN102876287-B
  • 发明人:   ZHANG T, ZHANG M, BO X, ZHOU Y, MEI Z, WANG Y, ZHU Y
  • 专利权人:   UNIV SOUTHEAST
  • 国际专利分类:   C01B013/14, C09K003/00
  • 专利详细信息:   CN102876287-A 16 Jan 2013 C09K-003/00 201330 Pages: 8 Chinese
  • 申请详细信息:   CN102876287-A CN10395414 17 Oct 2012
  • 优先权号:   CN10395414

▎ 摘  要

NOVELTY - A self-assembled laminated infrared film material is obtained by laminating a layered double hydroxide nanosheet and single layer of graphene oxide alternately. The number of layers in self-assembled laminated infrared film material is 2-40. The self-assembled laminated infrared film material has thickness of 2-200 nm. USE - Self-assembled laminated infrared film material (claimed). DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of self-assembled laminated infrared film material, which involves adding carboxylic acid solution of metallic ion (M1) and carboxylic acid solution of metallic ion (M2) to reactor and reacting for 4-10 hours under nitrogen atmosphere, adding inorganic alkaline aqueous solution, hydrothermal crystallizing for 48-72 hours, cooling, filtering, washing deionized water, dispersing layered double hydroxide by deionized water, immersing substrate in mixed solution of methanol and concentrated hydrochloric acid and adding concentrated sulfuric acid and heating modified substrate at room temperature for 5-15 minutes to obtain layered double hydroxide assembling substrate, adding aqueous solution of inorganic alkali to layered double hydroxide assembling substrate and assembling film materials.