• 专利标题:   Preparation of graphene and porous amorphous carbon film, involves placing cleaned metal nickel substrate in tubular furnace, heating with passage of hydrogen, flowing hydrocarbon, carrying out catalytic cracking, and forming film.
  • 专利号:   CN103613094-A, CN103613094-B
  • 发明人:   WEI H, YI L, ZHU D, LIU Y, YUAN L
  • 专利权人:   UNIV HUAZHONG SCI TECHNOLOGY
  • 国际专利分类:   C01B031/02, C01B031/04
  • 专利详细信息:   CN103613094-A 05 Mar 2014 C01B-031/04 201429 Pages: 10 Chinese
  • 申请详细信息:   CN103613094-A CN10624078 28 Nov 2013
  • 优先权号:   CN10624078

▎ 摘  要

NOVELTY - A metal nickel substrate is ultrasonically cleaned, dried, and placed in a tubular furnace. An inert gas is introduced into the furnace, and the substrate is heated is carried out at 750-1000 degrees C for 10-50 minutes with passage of hydrogen. A hydrocarbon is flown into the furnace at 20-100 sccm such that catalytic cracking of hydrocarbon is carried out and a graphene and amorphous carbon thin film is grown on the nickel substrate. The substrate is soaked in a corrosive etching liquid to obtain a graphene and porous amorphous carbon thin film. USE - Preparation of graphene and porous amorphous carbon film (claimed). ADVANTAGE - The method uses low-temperature conditions.