• 专利标题:   Preparation of shape memory epoxy foam composite material for shape memory plugging agent, involves mixing aqueous dispersion of nano particles with epoxy monomer, stirring to form Pickering emulsion and adding curing agent into pickering emulsion, pouring emulsion into mold, heating and curing.
  • 专利号:   CN114702722-A, CN114702722-B
  • 发明人:   QIN W, GU L, HE S, MA Q, ZHOU D, WU Y, FENG H, LIU L, XING X, LI Z
  • 专利权人:   BEIJING RES CENT CNOOC CHINA LTD, CNOOC CHINA LTD, CNOOC CHINA CO LTD
  • 国际专利分类:   C08G059/24, C08G059/30, C08G059/32, C08G059/42, C08G059/50, C08J009/28, C08K003/04, C08K003/22, C08L063/00, C08L063/02, C08L071/12, C08L073/00, C08L079/04, C09K008/42
  • 专利详细信息:   CN114702722-A 05 Jul 2022 C08J-009/28 202269 Chinese
  • 申请详细信息:   CN114702722-A CN10317476 29 Mar 2022
  • 优先权号:   CN10317476

▎ 摘  要

NOVELTY - Preparation of a high-temperature shape memory epoxy foam composite material involves: 1) mixing an aqueous dispersion of nano particles with an epoxy monomer, followed by stirring to form a Pickering emulsion of water in oil, and adding a curing agent into the pickering emulsion to form an emulsion; 2) pouring the emulsion into a mold, followed by heating and curing. USE - Method is used for preparing shape memory epoxy foam composite material usedstructure shape in shape memory plugging agent (claimed). ADVANTAGE - The preparation process involves using Pickering emulsion template to perform polymerization of epoxy monomer and curing agent, and simultaneously combines foaming and filler particle reinforcement mode, to prepare a shape memory ring having high transition temperature, high strength, toughness and high compressibility. The high-temperature shape memory foam composite material prepared, enables to meet the requirements of plugging in deep and high-temperature formations, and when used in plugging agent, the material enables to achieve crack plugging through its adaptive expansion, at high temperature. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: 1. shape memory epoxy foam composite. 2. shape memory plugging agent which is a granular material formed by cutting and pulverizing a sheet formed by pressing the shape memory epoxy foam composite material.