• 专利标题:   Ink preparation used for electronic information products involves preparing photosensitive graphene, mixing with photosensitive prepolymer, photoinitiator and reactive diluent and stirring.
  • 专利号:   CN105038412-A
  • 发明人:   LIU X, LUO J, LIU R, MA Q
  • 专利权人:   UNIV JIANGNAN
  • 国际专利分类:   C08F220/32, C08F226/12, C08F008/00, C09D011/03, C09D011/101, C09D011/52
  • 专利详细信息:   CN105038412-A 11 Nov 2015 C09D-011/52 201638 Pages: 6 Chinese
  • 申请详细信息:   CN105038412-A CN10557408 06 Sep 2015
  • 优先权号:   CN10557408

▎ 摘  要

NOVELTY - An ink preparation involves preparing photosensitive copolymer; dispersing graphene oxide in N,N-dimethyl formamide, adding hydrazine hydrate, reacting, cooling, adding photosensitive copolymer, dispersing in common solvent, cooling, centrifuging, washing and drying to get photosensitive graphene; and mixing photosensitive prepolymer, photoinitiator, reactive diluent and photosensitive graphene and stirring. USE - Method for preparing ink (claimed) used for electronic information products such as touch screen, radio-frequency identification and flexible circuits. ADVANTAGE - The ink has good thermal conductivity properties, low resistivity electronic circuit, large adhesion and high hardness. DETAILED DESCRIPTION - An ink preparation comprises dissolving glycidyl methacrylate, vinylcarbazole, azobisisobutyronitrile and solvent with stirring through nitrogen for 25-30 minutes, sealing, reacting at 50-100 degrees C for 8-16 hours, cooling to room temperature, adding acrylic acid or methacrylic acid, triphenylphosphine as catalyst and hydroquinone or resorcinol as polymerization inhibitor, reacting at 85-120 degrees C for 8-16 hours, precipitating and vacuum drying in oven at 20-80 degrees C to get photosensitive copolymer; dispersing graphene oxide in N,N-dimethyl formamide, adding hydrazine hydrate, reacting at 70-100 degrees C for 8-12 hours, cooling, adding photosensitive copolymer, dispersing in common solvent, cooling, centrifuging, washing and drying to get photosensitive graphene; and mixing 50-80 wt.% photosensitive prepolymer, 3-6 wt.% photoinitiator, 6-15 wt.% reactive diluent and 3.5-15 wt.% photosensitive graphene and stirring at room temperature.