• 专利标题:   Production of graphene oxide involves mixing graphite with strong acid, mixing with strong oxidizing agent, converting obtained exfoliated graphite oxide into graphene oxide by applying heat, removing residual materials, washing with water, and pulverizing into particles by vacuum-freeze-drying.
  • 专利号:   KR2483223-B1, WO2023120854-A1
  • 发明人:   SHIN T, HWANG G B, SHIN J, YOO J, SHIN T H, SHIN J H, YOO J H
  • 专利权人:   LAB M ZERO CO LTD
  • 国际专利分类:   C01B032/192, C01B032/194, C01B032/198
  • 专利详细信息:   KR2483223-B1 02 Jan 2023 C01B-032/198 202306 Pages: 20
  • 申请详细信息:   KR2483223-B1 KR185727 23 Dec 2021
  • 优先权号:   KR185727

▎ 摘  要

NOVELTY - Production of graphene oxide involves (i) mixing graphite with a strong acid to obtain a graphite oxide, (ii) exfoliating a layered structure of graphite oxide by mixing with a strong oxidizing agent, increasing the temperature to 20-25° C and stirring for 18-24 hours, (iii) converting the exfoliated graphite oxide into graphene oxide by applying heat at 40-55° C for 20-40 hours, (iv) removing residual materials other than graphene oxide synthesized through the conversion, (v) washing the solution containing the graphene oxide with deionized water and separating, and (vi) pulverizing the solution containing the graphene oxide into graphene oxide particles by vacuum-freeze-drying. USE - Production of graphene oxide. ADVANTAGE - The method enables large-scale production of graphene oxide, with controlled explosion caused by the strong oxidizing agent. The graphene oxide has a relatively higher oxidation degree than that of the existing graphene oxide, and a wide distribution of defects, so that various chemical reactions can be efficiently induced.