• 专利标题:   Manufacturing graphene nanofibers useful in energy conversion and storage applications comprises performing high temperature pyrolysis to hydrothermally treated cotton fiber and cotton rope, and characterizing obtained fibers by e.g. RAMAN.
  • 专利号:   AU2021100552-A4
  • 发明人:   PANDEY S, KARAKOTI M, DHALI S, KARKI N, SAHOO N G
  • 专利权人:   PANDEY S, KARAKOTI M, DHALI S, KARKI N, SAHOO N G
  • 国际专利分类:   B82Y035/00, B82Y040/00, C01B032/184
  • 专利详细信息:   AU2021100552-A4 29 Apr 2021 C01B-032/184 202141 Pages: 35 English
  • 申请详细信息:   AU2021100552-A4 AU100552 28 Jan 2021
  • 优先权号:   AU100552

▎ 摘  要

NOVELTY - Manufacturing graphene nanofibers (GNFs) from cotton sources comprises: selecting soft and fluffy stable cotton fiber (CF) and tenfold cotton rope (CR) upon investigating CFs and CR to synthesize GNFs of different shape and size; immersing stable CF and tenfold CR into solution of ethyl and isopropyl alcohols, where the alcohol-based solution is used to develop rapid carbon skeleton and flexibility within GNFs; pyrolyzing alcohol-soaked CF and CR upon placing inside hydrothermal reactor at 150 degrees C for 5 hours, nucleation of skeleton starts for growth of graphene nanosheets, performing high temperature pyrolysis to hydrothermally treated CF and CR inside tube furnace in inert atmosphere of nitrogen gas at 800 degrees C with heating rate of 5 degrees C/minutes of 40 minutes to develop graphitic nature with skeleton of CF and CR; and characterizing obtained GNFs by RAMAN, Fourier-transform infrared spectroscopy, field emission scanning electron microscopy (FESEM) analysis and UV-visible spectroscopy. USE - The process is useful for manufacturing graphene nanofibers (GNFs) from cotton sources, where the GNFs are useful in energy conversion and storage applications, and as active electrode materials for the smother passage of charge transportation in photovoltaic wires (all claimed). ADVANTAGE - The process: utilizes pyrolysis techniques to develop scalable and green synthesis of GNFs; shows the applicability of alcoholic mixtures to develop flexible GNFs; shows GNF based electrode for dye sensitized solar cell wires; and shows comparison of two types of the GNFs and evaluation of their band gaps to use them in the field of energy applications.