• 专利标题:   Preparation of bionic intelligent superhydrophobic graphene film involves mixing concentrated sulfuric acid with natural graphite, adding potassium permanganate, distilled water, hydrogen peroxide and diphenyl ether, and freeze-drying.
  • 专利号:   CN107140631-A, CN107140631-B
  • 发明人:   JIAO W, DING G, WANG R, HAO L, XU Z, LIU W, YANG F, HE X, YUAN Z, YANG S, KONG J
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   B82Y040/00, C01B032/184, C01B032/198
  • 专利详细信息:   CN107140631-A 08 Sep 2017 C01B-032/198 201773 Pages: 11 Chinese
  • 申请详细信息:   CN107140631-A CN10433707 09 Jun 2017
  • 优先权号:   CN10433707

▎ 摘  要

NOVELTY - The preparation method of bionic intelligent superhydrophobic graphene film involves adding 23 ml concentrated sulfuric acid with a concentration of 98 %mass and 1 g natural graphite to a beaker and then mixing, stirring the mixture, adding 6 g potassium permanganate to the mixture and then sintering, adding 80 ml distilled water to the mixture and then stirring, adding 60 ml distilled water and mixed solution (A) to the mixture and then centrifuging, adding 1 ml diphenyl ether to the mixture and then filtering using PTFE filter, and freeze-drying. USE - The method is useful for preparation of bionic intelligent superhydrophobic graphene film (claimed). ADVANTAGE - The method enables preparation of bionic intelligent superhydrophobic graphene film with excellent adsorption effect. DETAILED DESCRIPTION - The preparation method of bionic intelligent superhydrophobic graphene film involves adding 23 ml concentrated sulfuric acid with a concentration of 98 %mass and 1 g natural graphite to a beaker and then mixing, stirring the mixture, adding 6 g potassium permanganate to the mixture and then sintering, adding 80 ml distilled water to the mixture and then stirring, adding 60 ml distilled water and mixed solution (A) to the mixture and then centrifuging, adding 1 ml diphenyl ether to the mixture and then filtering using PTFE filter, and freeze-drying. The mixed solution (A) contains 10.81 ml hydrogen peroxide with a concentration of 30 %mass and 60 ml distilled water.