• 专利标题:   Preparation of graphene for e.g. supercapacitor, involves mixing graphite, potassium nitrate and potassium permanganate, adding concentrated sulfuric acid, isothermally oxidizing, pickling, washing, drying, extruding and reducing.
  • 专利号:   CN104051160-A
  • 发明人:   HU J, LI X, QI C, JIANG H
  • 专利权人:   DAYING JUNENG TECHNOLOGY DEV CO LTD
  • 国际专利分类:   H01G011/24, H01G011/36, H01G011/86
  • 专利详细信息:   CN104051160-A 17 Sep 2014 H01G-011/36 201482 Pages: 10 Chinese
  • 申请详细信息:   CN104051160-A CN10234762 30 May 2014
  • 优先权号:   CN10234762

▎ 摘  要

NOVELTY - Preparation of graphene involves mixing graphite, potassium nitrate and potassium permanganate in weight ratio of 1:0.5:3, stirring uniformly in a reaction vessel, adding 98% concentrated sulfuric acid, placing reaction vessel in a thermostatic chamber at low temperature, processing in three zones maintained at 0-4 degrees C, 35-45 degrees C and 80-100 degrees C, respectively, isothermally oxidizing at 80-100 degrees C, pickling oxidation product, washing, drying, extruding at 200-500 degrees C in air and reducing at 1000-1200 degrees C in inert gas atmosphere. USE - Preparation of graphene for supercapacitor and lithium ion battery. ADVANTAGE - Graphene having perfect crystalline microstructure is manufactured with high yield by simple method, and provides supercapacitor having excellent capacitance.