• 专利标题:   Preparing graphene film by batch comprises e.g. taking graphene oxide film as raw material, subjecting it to low-temperature heating for pretreatment, carrying out rolling treatment, performing heating treatment, and rolling.
  • 专利号:   CN112279239-A
  • 发明人:   LAO M, LU T, CHEN Y, NI K, LU H
  • 专利权人:   NINGBO HUAFENG PACKAGE CO LTD
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN112279239-A 29 Jan 2021 C01B-032/184 202119 Pages: 7 Chinese
  • 申请详细信息:   CN112279239-A CN10996746 21 Sep 2020
  • 优先权号:   CN10996746

▎ 摘  要

NOVELTY - Preparing graphene film by batch comprises (i) taking graphene oxide film as raw material, and subjecting it to low-temperature heating for pretreatment to obtain low-temperature pretreated graphene oxide film, (ii) carrying out rolling treatment of the low-temperature pretreated graphene oxide film, and performing medium-temperature heating treatment to obtain medium-temperature treated reduced graphene oxide film, (iii) carrying out rolling treatment of the medium -temperature-treated reduced graphene oxide film, and performing high-temperature heating treatment to obtain high-temperature-treated reduced graphene oxide film, and (iv) rolling the reduced graphene oxide film under high temperature treatment to obtain final product. USE - The method is useful for preparing graphene film by batch. ADVANTAGE - The method: is simple; reduces the residual oxygen-containing group in the graphene film; improves graphene film performance; reduces the graphene film interlayer gap; and improves the graphene film surface flatness. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene film prepared by above method.