• 专利标题:   Preparing nanocomposite, by washing wet graphene with tetraoxyfuran, dissolving polylactic acid in tetrahydrofuran by mechanical stirring, dispersing graphite in tetrahydrofuran, ultrasonically treating, pulling film, crushing and drying.
  • 专利号:   CN110862656-A
  • 发明人:   ZHI T
  • 专利权人:   ZHI T
  • 国际专利分类:   C08J003/215, C08K003/04, C08L067/04
  • 专利详细信息:   CN110862656-A 06 Mar 2020 C08L-067/04 202026 Pages: 5 Chinese
  • 申请详细信息:   CN110862656-A CN10986926 28 Aug 2018
  • 优先权号:   CN10986926

▎ 摘  要

NOVELTY - Method for preparing graphene/polylactic acid nanocomposite, involves (i) washing wet graphene with tetraoxyfuran for 5 times to remove water content, (ii) dissolving polylactic acid (4 g polylactic acid corresponding to 1 g graphene) in tetrahydrofuran by mechanical stirring (1 g polylactic acid corresponding to 10 ml tetrahydrofuran), (iii) dispersing dilute graphite in tetrahydrofuran (1 g graphite corresponding to 40 ml tetrahydrofuran) in three-necked flask by mechanical stirring, ultrasonically treating and stirring for 2-3 hours until pulsate becomes thick, and (iv) adding polylactic acid solution to graphite/tetrahydrofuran mixed solution, continuously ultrasonically treating and mechanically stirring for 4 hours, pouring mixture to open container, drying in oven at 50 degrees C for 10 hours, properly pulling film on surface, so that solvent evaporates, crushing into particles or powders and drying in vacuum oven at 8 degrees C for 6 hours to obtain graphene/polylactic acid master batch. USE - The method is useful for preparing graphene/polylactic acid nanocomposite. ADVANTAGE - The method has simple operation and easy temperature control.